反応 #61206

反応方程式

N-(2-iodo-4-nitro-5-trifluoromethyl-phenyl)-methanesulfonamide

2-methyl-1-buten-3-yne

→

title compound

2-Isopropenyl-1-methanesulfonyl-5-nitro-6-trifluoromethyl-1H-indole

反応条件

後処理

1. 1
   その他This compound-was prepared

実験手順

This compound-was prepared using the general Sonagashira conditions as described in general Example C, starting from N-(2-iodo-4-nitro-5-trifluoromethyl-phenyl)-methanesulfonamide (9.0 g, 21.9 mmol) and 2-methyl-1-buten-3-yne (6.25 mL, 65.7 mmol) to yield the title compound as a reddish-brown solid.

出典