反応 #6119

反応方程式

2-bromo-3,5-dicyanobenzonitrile

sodium thiomethylate

→

expected product

3,5-dicyano-2-mercaptobenzonitrile

反応条件

後処理

1. 1
   その他If the procedure described in Preparation LV

実験手順

If the procedure described in Preparation LV is followed starting from 6 g (26.10-3 mol) of 2-bromo-3,5-dicyanobenzonitrile and 6 g (86.10-3 mol) of sodium thiomethylate, 6 g (quantitative yield) of the expected product are obtained in the form of an oil.

出典