反応 #6109

反応方程式

dimethylthiocarbamoyl chloride

2-tri-fluoromethylphenol

potassium hydroxide

→

yellow oil

収率 89.0%

O-2-trifluoromethylphenyl dimethylthiocarbamate

収率 89.0%

反応条件

実験手順

If the procedure described in Preparation XI is followed starting from 3.95 g (24.3.10-3 mol) of 2-tri-fluoromethylphenol, 1.43 g (25.6.10-3 mol) of potassium hydroxide and 3.46 g (28.10-3 mol) of dimethylthiocarbamoyl chloride, 5.37 g (yield: 89%) of a yellow oil are obtained.

出典