反応 #610117

反応方程式

1,8-dichloroanthraquinone

N,N-dimethylethylenediamine

→

Compound 6

1,8-bis(2-(dimethylamino)ethylamino)anthracene-9,10-dione

溶媒

water

反応条件

後処理

1. 1
   温度was refluxed for 18 h
2. 2
   その他to precipitate the title compound which
3. 3
   その他was recrystallised from methanol

実験手順

A mixture of 1,8-dichloroanthraquinone (5.5 g, 20 mmol) and N,N-dimethylethylenediamine (40 mL) was refluxed for 18 h. The mixture was cooled to room temperature and diluted with water to precipitate the title compound which was recrystallised from methanol to afford Compound 6 (4.5 g). The structure of Compound 6 is given below:

出典