反応 #6100

反応方程式

potassium hydroxide

2-hydroxybenzonitrile

dimethylthiocarbamoyl chloride

→

expected product

収率 94.0%

O-2-cyanophenyl dimethylthiocarbamate

収率 94.0%

反応条件

実験手順

If the procedure described in Preparation XVI is followed starting from 15 g (126.10-3 mol) of 2-hydroxybenzonitrile, 17.9 g (145.10-3 mol) of dimethylthiocarbamoyl chloride and 7.4 g (126.10-3 mol) of potassium hydroxide, 24.1 g (yield: 94%) of the expected product are obtained.

出典