反応 #6097

反応方程式

potassium hydroxide

3-hydroxybenzonitrile

dimethylthiocarbamoyl chloride

→

expected product

O-3-cyanophenyl dimethylthiocarbamate

反応条件

実験手順

If the procedure described in Preparation XI is followed starting from 15 g (126.10-3 mol) of 3-hydroxybenzonitrile, 17.9 g (145.10-3 mol) of dimethylthiocarbamoyl chloride and 7.4 g (132.10-3 mol) of potassium hydroxide, 29 g (quantitative yield) of the expected product are obtained.

出典