反応 #60952

反応方程式

2-Chloro-5-methylsulfamoyl-benzoic acid

2-Chloro-5-sulfino-benzoic acid

pyrrolidine

→

title compound

収率 91.0%

2-Chloro-5-(pyrrolidine-1-sulfonyl)-benzoic acid

収率 91.0%

反応条件

後処理

1. 1
   その他obtained in 91% yield

実験手順

The title compound was synthesised according to the procedure described for 2-Chloro-5-methylsulfamoyl-benzoic acid from 2-Chloro-5-sulfino-benzoic acid and pyrrolidine and obtained in 91% yield. MS (m/e): 288.0 (MH−, 100%).

出典