反応 #60949

ord-7ecdec9311564fbe9bd5e74868616de1

反応条件

詳細条件
See reaction.notes.procedure_details.

後処理

  1. 1
    その他obtained in 78% yield

実験手順

The title compound was synthesised according to the procedure described for 2-Chloro-5-methylsulfamoyl-benzoic acid from 2-Chloro-5-sulfino-benzoic acid and ethylamine and obtained in 78% yield. MS (m/e): 262.2 (MH−, 100%).

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US07427612B2uspto-grants-2008_09