反応 #60758

ord-b57bcbbc48ad42beb51c475a615ded38

反応方程式

O=C=NC1CCCCC1
cyclohexyl isocyanate
[N-]=C=O
isocyanate
NC1=c2ccoc2=NCN1c1cccc(N)c1
4-Amino-3-(3-aminophenyl)furo[2,3-d]pyrimidine
NC1=c2ccoc2=NCN1c1cccc(NC(=O)NC2CCCCC2)c1
4-Amino-3-(3-((cyclohexyl)aminocarbonylamino)phenyl)furo[2,3-d]pyrimidine

反応条件

詳細条件
See reaction.notes.procedure_details.

後処理

  1. 1
    その他The compound was prepared

実験手順

The compound was prepared following the procedure described in Example 232(b), using cyclohexyl isocyanate as the isocyanate of choice, and 4-Amino-3-(3-aminophenyl)furo[2,3-d]pyrimidine (10) as the diamine of choice. MS(ES) m/e 352 [M+H]+.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US07427623B2uspto-grants-2008_09