反応 #59920

反応方程式

( 6f )

2-(((4-((2-methoxy-1,3-dioxan-5-yl)methoxy)-3-methylpyridin-2-yl)methyl)sulfinyl)-1H-benzimidazole sodium salt

1,3-dioxan-2-ylmethanol

→

title compound

収率 10.0%

2-(((4-(1,3-dioxan-2-ylmethoxy)-3-methylpyridin-2-yl)methyl)sulfinyl)-1H-benzimidazole sodium salt

収率 10.0%

反応条件

後処理

1. 1
   その他obtained in the step (32b)

実験手順

The same procedure as in the steps (6b) to (6f) of Example 6 was repeated using 1,3-dioxan-2-ylmethanol obtained in the step (32b) to obtain the title compound (148 mg, total yield:10%) as a light yellow solid.

出典