反応 #59918

反応方程式

( 8g )

2-(((3-methyl-4-(2-(2-propyl-1,3-dioxan-2-yl)ethoxy)pyridin-2-yl)methyl)sulfinyl)-1H-benzimidazole sodium salt

2-(2-methyl-1,3-dioxan-2-yl)ethanol

→

title compound

収率 2.5%

2-(((3-methyl-4-(2-(2-methyl-1,3-dioxan-2-yl)ethoxy)pyridin-2-yl)methyl)sulfinyl)-1H-benzimidazole sodium salt

収率 2.5%

反応条件

後処理

1. 1
   その他obtained in the step (30a)

実験手順

The same procedure as in the steps (8c) to (8g) of Example 8, was repeated using 2-(2-methyl-1,3-dioxan-2-yl)ethanol obtained in the step (30a) to obtain the title compound (113 mg, total yield: 2.5%) as a light yellow solid.

出典