反応 #59911

反応方程式

2-(hydroxymethyl)-1,3-propanediol

cyclohexanone

→

title compound

収率 65.0%

1,5-dioxaspiro[5.5]undec-3-ylmethanol

収率 65.0%

反応条件

実験手順

The same procedure as in the step (1a) of Example 1 was repeated using 2-(hydroxymethyl)-1,3-propanediol and cyclohexanone to obtain the title compound (2.26 g, yield: 65%) as a light yellow oil.

出典