反応 #595369

反応方程式

methyl 4-(benzyloxy)-2-(prop-1-en-2-yl)benzoate

→

title compound

methyl 4-hydroxy-2-isopropylbenzoate

溶媒

methanol

反応条件

後処理

1. 1
   ろ過Then the mixture was filtered
2. 2
   濃縮the filtrate was concentrated

実験手順

To a solution of methyl 4-(benzyloxy)-2-(prop-1-en-2-yl)benzoate (i-1d) (4.6 g, 16.3 mmol) in methanol (100 ml) was added Pd/C (0.46 g). The mixture was stirred at rt under H2 atmosphere for 24 h. Then the mixture was filtered, and the filtrate was concentrated to afford the title compound. LCMS (ESI) calc'd for C11H14O3 [M+H]+: 195.1. found: 195.1.

出典