反応 #59296

反応方程式

(S)-7-Amino-5-(2-methoxy-ethyl)-5H,7H-dibenzo[b,d]azepin-6-one

malonic acid monoethyl ester

→

title compound

N—[(S)-5-(2-Methoxy-ethyl)-6-oxo-6,7-dihydro-5H-dibenzo[b,d]azepin-7-yl]-malonamic acid ethyl ester

反応条件

実験手順

Using (S)-7-Amino-5-(2-methoxy-ethyl)-5H,7H-dibenzo[b,d]azepin-6-one and malonic acid monoethyl ester, the title compound was prepared in the same manner as described for example 1c. Colorless, viscous oil (>98%). MS: m/e=397(M+H+).

出典