反応 #58290

ord-a7452d63123c42d1972cb33cffe8ea84

反応条件

詳細条件
See reaction.notes.procedure_details.

後処理

  1. 1
    その他This compound is synthesized
  2. 2
    その他The product is crystallized from diisopropyl ether

実験手順

This compound is synthesized according to the method described in 3.2. by reacting 2-bromo-5-methoxybenzoic acid pretreated with n-butyllithium with N-methoxy-4-methoxymethyl-N-methylbenzamide. The product is crystallized from diisopropyl ether.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US07423030B2uspto-grants-2008_09