反応 #58261

ord-67d0165016824c9f88d8389d83c0600b

反応方程式

COc1ccc(C(=O)c2ccc3c(c2)OCO3)c(C(=O)O)c1
2-(1,3-benzodioxol-5-yl)carbonyl-5-methoxybenzoic acid
NN.O
hydrazine hydrate
→
COc1ccc2c(-c3ccc4c(c3)OCO4)n[nH]c(=O)c2c1
4-(1,3-Benzodioxol-5-yl)-7-methoxy-2H-phthalazin-1-one

反応物

COc1ccc(C(=O)c2ccc3c(c2)OCO3)c(C(=O)O)c1
2-(1,3-benzodioxol-5-yl)carbonyl-5-methoxybenzoic acid
NN.O
hydrazine hydrate

試薬

なし

反応条件

詳細条件
See reaction.notes.procedure_details.

後処理

  1. 1
    その他This compound is obtained

実験手順

This compound is obtained according to the procedure described in 1.2. by reacting 2-(1,3-benzodioxol-5-yl)carbonyl-5-methoxybenzoic acid unpurified with hydrazine hydrate.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US07423030B2uspto-grants-2008_09