反応 #578433

反応方程式

4-bromostyrene

acrolein

methacrylate

AIBN

PGMEA

→

bromostyrene acrolein methacrylate

反応条件

後処理

1. 1
   その他The mixture was polymerized
2. 2
   その他After completion of the polymerization
3. 3
   その他the polymerization product was precipitated in n-hexane
4. 4
   ろ過filtered
5. 5
   その他dried in vacuo

実験手順

3 g of 4-bromostyrene, 4 g of acrolein, 3 g of methacrylate and 0.2 g of AIBN were sufficiently mixed with 50 g of PGMEA. The mixture was polymerized by heating the mixture at 67° C. for 8 hours. After completion of the polymerization, the polymerization product was precipitated in n-hexane, filtered, and dried in vacuo to give a poly(bromostyrene-acrolein-methacrylate) copolymer.

出典