反応 #5713

反応方程式

dimethyldichlorosilane

ammonia

→

hexamethylcyclotrisilazane

溶媒

benzene

反応条件

後処理

1. 1
   その他at 30° C.
2. 2
   その他removing ammonia chloride by-product
3. 3
   ろ過by filtration through a glass
4. 4
   ろ過filter
5. 5
   workup.DISTILLATIONthe like, and distilling the reaction product

実験手順

This method involves reacting dimethyldichlorosilane with ammonia in benzene at 30° C., removing ammonia chloride by-product by filtration through a glass filter or the like, and distilling the reaction product to isolate hexamethylcyclotrisilazane.

出典