反応 #568463

ord-71a2ee2334544128819ed44cb8c0e960

反応方程式

CC(C)N
isopropylamine
O=C(O)CNCP(=O)(O)O
glyphosate
CC(C)N
isopropylarnine
O=C(O)CNCP(=O)(O)O
glyphosate
O=C(O)CNCP(=O)(O)O
glyphosate
→
CC(C)N.O=C(O)CNCP(=O)(O)O
glyphosate isopropylamine

反応物

CC(C)N
isopropylamine
O=C(O)CNCP(=O)(O)O
glyphosate
CC(C)N
isopropylarnine
O=C(O)CNCP(=O)(O)O
glyphosate
O=C(O)CNCP(=O)(O)O
glyphosate

試薬

なし

溶媒

O
water
O
water

反応条件

詳細条件
See reaction.notes.procedure_details.

後処理

  1. 1
    温度with heat generation
  2. 2
    workup.STIRRINGstirring

実験手順

41.86 parts of glyphosate having a purity of 95.57% were added to 42.40 parts of water. When 13.99 parts of isopropylarnine were added to the mixture, with stirring, the glyphosate started to dissolve in the water with heat generation. A further 1.75 parts of isopropylamine were then added to the mixture and stirring was continued. As a result, the glyphosate dissolved completely to give a glyphosate-isopropylamine solution containing 40.01 parts of glyphosate.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US05789345uspto-grants-1998_08