反応 #565305

ord-cac7dc5fbc6f4ffc85425c4077b9a4ad

溶媒

反応条件

詳細条件
See reaction.notes.procedure_details.

後処理

  1. 1
    workup.ADDITIONwere mixed together

実験手順

7.31 parts by weight of resorcin and 10.77 parts by of formalin (having a concentration of 37% by weight) were mixed together. An aqueous solution of sodium hydroxide (containing 0.33 parts by weight of sodium hydroxide) was added to the resulting mixture and stirred. Thereafter 160.91 parts by weight of water were added and the mixture was aged for 5 hours to provide an aqueous solution of resorcin-formalin resin (resorcin-formalin primary condensate, referred to RF) having a solid content of 6.40 % by weight.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US06641905B1uspto-grants-2003_11