反応 #56164

ord-6c4f0f1cc97a4a29b2cfbcd3fb98a8f7

反応条件

詳細条件
See reaction.notes.procedure_details.

実験手順

1,8-Diaminonaphthalene (1.04 grams; 0.00656 mole) and p-pentafluoroethoxybenzoyl chloride (1.8 grams; 0.00656 mole) were reacted in the procedures of Example 3, yielding 2.25 grams of product (82.7% yield), m.p., 240° C. (dec.), mass spectrum m/e 378.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US04224326uspto-grants-1980_09