反応 #56163

反応方程式

1,8-Diaminonaphthalene

p-Trifluoromethoxybenzoyl fluoride

→

2-(p-TRIFLUOROMETHOXYPHENYL)-1H-PERIMIDINE HYDROFLUORIDE

溶媒

toluene

toluene

反応条件

後処理

1. 1
   その他of toluene, then decanted
2. 2
   workup.ADDITIONBoth solutions were added simultaneously to 25 ml

実験手順

1,8-Diaminonaphthalene (1.52 grams; 0.0096 mole) was dissolved in 25 ml. of toluene, then decanted. p-Trifluoromethoxybenzoyl fluoride (2.0 grams; 0.0096 mole) was dissolved in 25 ml. of toluene. Both solutions were added simultaneously to 25 ml. of toluene. After the reaction mixture had been stirred for approximately 4 hours, TLC indicated that the reaction was complete.

出典