反応 #56162

反応方程式

1,8-Diaminonaphthalene

m-trifluoromethylbenzoyl chloride

→

2-(m-trifluoromethylphenyl)-1H-perimidine hydrochloride

収率 95.4%

反応条件

後処理

1. 1
   その他yielding 33.3 g

実験手順

1,8-Diaminonaphthalene (15.82 g.; 0.10 mole) and m-trifluoromethylbenzoyl chloride (20.8 g.; 0.10 mole) were reacted in the same procedures as reported in Example 1, yielding 33.3 g. (95.4% yield) of 2-(m-trifluoromethylphenyl)-1H-perimidine hydrochloride, m.p. 280° C. (dec), mass spectrum m/e 312.

出典