反応 #56152

反応方程式

isostearic acid

triethylamine

→

2-octyl dodecyl ether

反応条件

後処理

1. 1
   workup.ADDITIONthere are slowly added

実験手順

To 32 g (0.1 mole) of isostearic acid there is added 0.3 ml (0.002 mole) of triethylamine. The resulting mixture is heated to 130° C. under a nitrogen atmosphere and there are slowly added thereto 40 g (0.1 mole) of 2-octyl dodecyl ether of glycidyl obtained according to the above method. After heating for 3 hours and 15 minutes at 130° C., the amount of the reaction determined by acid index is 93%.

出典