反応 #56111

ord-414dbc5005a144c69fd585ed4937b365

反応方程式

C=C(C)C(=O)OCCN(C)C
DMAEMA
CC(=O)O
acetic acid
C=C(C)C(=O)OCCN(C)C
DMAEMA
C=CC(N)=O
acrylamide
C=CC(N)=O
acrylamide
→
C=C(C)C(=O)OCCN(C)C.C=CC(N)=O
Acrylamide DMAEMA

反応物

C=C(C)C(=O)OCCN(C)C
DMAEMA
CC(=O)O
acetic acid
C=C(C)C(=O)OCCN(C)C
DMAEMA
C=CC(N)=O
acrylamide
C=CC(N)=O
acrylamide

試薬

なし

溶媒

O
water

反応条件

詳細条件
See reaction.notes.procedure_details.

後処理

  1. 1
    その他was recovered

実験手順

To a solution of 50.0 grams of acetic acid in 350 grams of water is added 131 grams of DMAEMA followed by 119 grams of acrylamide. The pH of the solution is 7.0 without any adjustment. The rest of the procedure is the same as followed in Example A. After 5 hours G.L.C. analysis showed there was no DMAEMA monomer remaining, while 33% of the acrylamide was recovered. This indicates that ≈66% of the DMAEMA had been quaternized.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US04224150uspto-grants-1980_09