反応 #56110

反応方程式

DMAEMA

acetic acid

DMAEMA

acrylamide

acrylamide

→

Acrylamide DMAEMA

溶媒

water

反応条件

後処理

1. 1
   その他was recovered which
2. 2
   workup.WAITA small sample of the monomer solution was stored for 24 hours at 25° C

実験手順

To a solution of 40 grams of acetic acid in 350 grams of water is added 131 grams of DMAEMA followed by 119 grams of acrylamide. The pH is 7.7. The rest of the procedure is the same or that followed in Example A. After 5 hours g.l.c. analysis showed no DMAEMA present while 49.5% of the acrylamide was recovered which indicates that ≈99% of the DMAEMA had been quaternized. A small sample of the monomer solution was stored for 24 hours at 25° C. The NMR spectrum showed that 73% of the DMAEMA had been quaternized.

出典