反応 #56102

ord-2dd6a601e2ae4d81ba19de47225e3306

反応方程式

Nc1c([N+](=O)[O-])ccc2ccccc12
1-amino-2-nitronaphthalene
Nc1ccc([N+](=O)[O-])c2ccccc12
1-amino-4-nitronaphthalene
→
CC1(C)Nc2cccc3c(N=Nc4c([N+](=O)[O-])ccc5ccccc45)ccc(c23)N1
desired compound
CC1(C)Nc2cccc3c(N=Nc4c([N+](=O)[O-])ccc5ccccc45)ccc(c23)N1
2,3-Dihydro-2,2-Dimethyl-6-(2-Nitronaphthylazo)Perimidine

反応物

Nc1c([N+](=O)[O-])ccc2ccccc12
1-amino-2-nitronaphthalene
Nc1ccc([N+](=O)[O-])c2ccccc12
1-amino-4-nitronaphthalene

試薬

なし

反応条件

詳細条件
See reaction.notes.procedure_details.

実験手順

In the manner described in Example 8, substituting 9.5 grams of 1-amino-2-nitronaphthalene for the 1-amino-4-nitronaphthalene, the desired compound is obtained.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US04224071uspto-grants-1980_09