反応 #55534

ord-187aeb1e582644feb735ebd3aedb8f97

反応方程式

NC(=O)[O-]
carbamate
NC(=O)Cl
carbamic acid chloride
O=C=Nc1cc(Cl)cc(Cl)c1
3,5-dichlorophenyl isocyanate
[N-]=C=O
isocyanate
COC(=O)Nc1cc(Cl)cc(Cl)c1
methyl N-(3,5-dichlorophenyl)-carbamate

反応条件

詳細条件
See reaction.notes.procedure_details.

後処理

  1. 1
    その他is obtained

実験手順

The carbamate used as the starting material is obtained by reacting an isocyanate with an alcohol or a carbamic acid chloride with an alcohol in the presence of an alkali, in the conventional manner. For example, reaction of 3,5-dichlorophenyl isocyanate with methyl alcohol gives methyl N-(3,5-dichlorophenyl)-carbamate (melting point 121° C.).

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US04220787uspto-grants-1980_09