反応 #55413
ord-8f9a7f77cbff44b4b91123068a7ced40
反応条件
詳細条件
See reaction.notes.procedure_details.
実験手順
Methyl 10-carboxydecyldithiocarbamate (28 g., 0.096 mol.) was reacted with 6.5 g. (0.1 mol.) of sodium azide according to the procedure described in Example 7. Acidification upon work-up gave 1-(10-carboxydecyl)tetrazole-5-thiol as a white precipitate, m.p. 95°-98°.