反応 #55386

反応方程式

3-mercapto-1,2,4-triazole

3-aminopropanol

hydrobromic acid

→

3-(3-aminopropylthio)-1,2,4-triazole dihydrobromide

反応条件

後処理

1. 1
   温度under reflux for 24 hours
2. 2
   その他The reaction mixture is evaporated to dryness
3. 3
   その他the residue recrystallised from ethanol/ether

実験手順

A solution of 3-mercapto-1,2,4-triazole and 3-aminopropanol in hydrobromic acid is heated under reflux for 24 hours. The reaction mixture is evaporated to dryness and the residue recrystallised from ethanol/ether to give 3-(3-aminopropylthio)-1,2,4-triazole dihydrobromide.

出典