反応 #55334

ord-7dbf822835bd4ba1b6edb635d46894d6

反応条件

詳細条件
See reaction.notes.procedure_details.

実験手順

185 g of glycerol epichlorhydrin are reacted with one mole, i.e., 186 g of dodecanol at 75°-80° C. in the presence of 1.5 ml of an acetic acid complex containing 36% BF3. Dodecyl ether of polyepichlorohydrin having the following formula is obtained:

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US04220602uspto-grants-1980_09