反応 #55239

反応方程式

hydrogen

N-[[2-[3-(dimethylamino)propoxy]phenyl]methyl]-N-[2-(4-nitrophenyl)ethyl]-3-phenyl-2-propenamide, oxalate salt

hydrogen

→

title compound

N-[2-(4-Aminophenyl)ethyl]-N-[[2-[3-(dimethylamino)propoxy]phenyl]methyl]-3-phenyl-2-propenamide, oxalate salt

溶媒

ethanol

反応条件

後処理

1. 1
   その他is consumed
2. 2
   ろ過filtered
3. 3
   その他the solvent evaporated under reduced pressure

実験手順

A suspension of 10 parts of N-[[2-[3-(dimethylamino)propoxy]phenyl]methyl]-N-[2-(4-nitrophenyl)ethyl]-3-phenyl-2-propenamide, oxalate salt (1:1) in 100 ml of ethanol is treated with 1 part of 5% palladium on carbon and placed under 3 atmospheres of gaseous hydrogen. The mixture is shaken until one equivalent of hydrogen is consumed, filtered and the solvent evaporated under reduced pressure to give the title compound.

出典