反応 #55199

反応方程式

3-(2',4'-difluoro-4-biphenylyl)-2-butenoic acid

diazomethane

→

3-(2',4'-difluoro-4-biphenylyl)-2-butenoic acid methyl ester

溶媒

THF

反応条件

後処理

1. 1
   その他the mixture is evaporated

実験手順

1 g. of 3-(2',4'-difluoro-4-biphenylyl)-2-butenoic acid is dissolved in 10 ml. of THF and an ethereal solution of diazomethane is added dropwise, with stirring, until no further evolution of nitrogen is observed. After 20 minutes, the mixture is evaporated to give 3-(2',4'-difluoro-4-biphenylyl)-2-butenoic acid methyl ester, m.p. 90°-92°.

出典