反応 #55061

反応方程式

rac.-3-tert. butoxy-2-methyl-1-propanol

bromine triphenylphosphine

→

rac.-3-tert. butoxy-2-methyl-1-bromopropane

収率 35.0%

反応条件

実験手順

Reaction of rac.-3-tert. butoxy-2-methyl-1-propanol with bromine-triphenylphosphine using the procedure of Example 28 gave rac.-3-tert. butoxy-2-methyl-1-bromopropane in 35% yield as a colorless liquid, b.p. 67°-77° C. (bath temperature) (9 mm Hg.).

出典