反応 #550375

ord-9e89be64e68542f68f6dab234b76f342

反応方程式

CC1(C)OC(=O)Nc2cc(OCCCCOS(C)(=O)=O)ccc21
7-(4-methanesulfonyloxy-butoxy)-4,4-dimethyl-4H-3,1-benzoxazin-2-one
Sc1ccccn1
2-mercapto-pyridine
→
CC1(C)OC(=O)Nc2cc(OCCCCSc3ccccn3)ccc21
7-[4-(2-Pyridylmercapto)-butoxy]-4,4-dimethyl-4H-3,1-benzoxazin-2-one

反応物

CC1(C)OC(=O)Nc2cc(OCCCCOS(C)(=O)=O)ccc21
7-(4-methanesulfonyloxy-butoxy)-4,4-dimethyl-4H-3,1-benzoxazin-2-one
Sc1ccccn1
2-mercapto-pyridine

試薬

なし

反応条件

詳細条件
See reaction.notes.procedure_details.

実験手順

Prepared analogously to Example 210 from 7-(4-methanesulfonyloxy-butoxy)-4,4-dimethyl-4H-3,1-benzoxazin-2-one and 2-mercapto-pyridine.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US04518597uspto-grants-1985_05