反応 #550223

反応方程式

crotonyl chloride

carnitine hydrochloride

ethyl ether

→

crotonoyl carnitine

溶媒

trifluoroacetic acid

反応条件

後処理

1. 1
   その他a precipitate formed
2. 2
   ろ過The precipitate was filtered off
3. 3
   その他such in the subsequent reaction

実験手順

8 cc (0.08 moles) of crotonyl chloride were added to a solution of carnitine hydrochloride (8 grams; 0.04 moles) in trifluoroacetic acid. The reaction mixture was kept under stirring at 50° C. overnight. Subsequently, ethyl ether was added to the mixture and a precipitate formed. The precipitate was filtered off and used as such in the subsequent reaction.

出典