反応 #550221

ord-8e70316d801d434dbee9c65ee24d87c5

反応方程式

C[N+](C)(C)CC(O)(CC(=O)[O-])C(=O)CCBr
bromopropionyl carnitine
→
C=CC(=O)C(O)(CC(=O)[O-])C[N+](C)(C)C
acryloyl carnitine

反応物

C[N+](C)(C)CC(O)(CC(=O)[O-])C(=O)CCBr
bromopropionyl carnitine

試薬

なし

溶媒

O
H2O

反応条件

詳細条件
See reaction.notes.procedure_details.

後処理

  1. 1
    workup.ADDITIONwere added
  2. 2
    ろ過filtered

実験手順

To a solution of 4 grams of bromopropionyl carnitine in 40 ml of H2O 100 cc of IR 45 amberlite resin activated in OH form were added. The reaction mixture was kept under stirring for 2 hours, then filtered and lyophilized.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US04518613uspto-grants-1985_05