反応 #55013

反応方程式

ethyl 4-oxo-1-piperidinecarboxylate

2-pyrimidinamine

methylbenzene

→

ethyl 4-(2-pyrimidinylimino)-1-piperidinecarboxylate

溶媒

water

反応条件

後処理

1. 1
   その他The reaction mixture is evaporated

実験手順

A mixture of 34 parts of ethyl 4-oxo-1-piperidinecarboxylate, 20 parts of 2-pyrimidinamine, 8 drops of acetic acid and 90 parts of methylbenzene is stirred and refluxed for 28 hours with water-separator. The reaction mixture is evaporated, yielding 50 parts of ethyl 4-(2-pyrimidinylimino)-1-piperidinecarboxylate as a residue.

出典