反応 #547696

ord-ce31d14f9f8a4b9b94c8ad63820d9d9b

反応方程式

Cc1ccc(Nc2cc(O)ccc2[N+](=O)[O-])cc1
3-(4-methylphenyl)amino-4-nitrophenol
COC(=O)CCCCCBr
6-bromohexanoic acid methyl ester
→
COC(=O)CCCCCOc1ccc([N+](=O)[O-])c(Nc2ccc(C)cc2)c1
6-[3-(4-Methylphenyl)amino-4-nitrophenyl]oxyhexanoic acid methyl ester

反応物

Cc1ccc(Nc2cc(O)ccc2[N+](=O)[O-])cc1
3-(4-methylphenyl)amino-4-nitrophenol
COC(=O)CCCCCBr
6-bromohexanoic acid methyl ester

試薬

なし

反応条件

詳細条件
See reaction.notes.procedure_details.

後処理

  1. 1
    その他1.5 g was obtained

実験手順

990 mg of 3-(4-methylphenyl)amino-4-nitrophenol was reacted with 6-bromohexanoic acid methyl ester according to general operating instructions 2. 1.5 g was obtained.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US07196202B2uspto-grants-2007_03