反応 #54543

反応方程式

dimethylphenethylamine

lithium

ammonia

→

1-[2-(dimethylamino)ethyl]-1,4-cyclohexadiene

溶媒

ethanol

反応条件

実験手順

45 g. (0.3 moles) of the dimethylphenethylamine is reduced by treatment with 16 g. of lithium (2.3 g. atom) in 1.5 l. of ammonia and 250 ml. of ethanol according to the procedure of Example 1(a) to yield crude 1-[2-(dimethylamino)ethyl]-1,4-cyclohexadiene.

出典