反応 #54526

反応方程式

cyclohexene oxide

dimethylamine

hydrochloride

→

trans-2-Dimethylaminocyclohexanol

溶媒

benzene

反応条件

後処理

1. 1
   その他67, 63899 d, Rocz

実験手順

This compound was previously prepared from cyclohexene oxide and dimethylamine in benzene at room temperature for 14 days in 95% yield, b.p. 90° (20 mm): J. Chem. Soc., 4835 (1965); or in autoclave: C. A. 67, 63899 d, Rocz. Chem. 41, 541 (1967) b.p. 88° (14 mm); also Bull. Soc. Chim. France, 850 (1947): hydrochloride and resolution reported.

出典