反応 #544432

ord-f2b98b38f7104dd097424cd92de5d75b

反応方程式

CCCCOP(=O)(OCCCC)OCCCC
tributyl phosphate
CC(O)C(=O)[O-].[NH4+]
ammonium lactate
CC(O)C(=O)[O-].[NH4+]
ammonium lactate
CC(O)C(=O)O
lactic acid

反応条件

詳細条件
See reaction.notes.procedure_details.

後処理

  1. 1
    温度The reaction mixture was heated for 0.5 hour at 110–118° C.

実験手順

The procedure described in Example 1 was followed except that 7.57 g of a 70% solution of ammonium lactate was combined with 50 g tributyl phosphate. The reaction mixture was heated for 0.5 hour at 110–118° C. and a reduced pressure of 4.5–5.5 mm Hg, resulting in a conversion of about 97% from ammonium lactate to lactic acid.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US07186856B2uspto-grants-2007_03