反応 #54250

反応方程式

isobutyraldehyde

benzhydrylamine

benzene

→

isobutylidenebenzhydrylamine

溶媒

water

反応条件

後処理

1. 1
   温度The cloudy mixture was heated
2. 2
   温度On cooling the solution
3. 3
   ろ過was filtered
4. 4
   その他to remove a small amount of solid
5. 5
   その他evaporated

実験手順

14.4 parts of isobutyraldehyde was added to 36.6 parts of benzhydrylamine in 100 parts of dry benzene at room temperature with stirring. The cloudy mixture was heated to reflux with water-separation for 4 hours. On cooling the solution was filtered to remove a small amount of solid and evaporated to give isobutylidenebenzhydrylamine.

出典