反応 #54199

ord-a234627dec74419db08ec114ddbb8683

反応条件

詳細条件
See reaction.notes.procedure_details.

後処理

  1. 1
    workup.DISTILLATIONof a 40% aqueous solution), distilled water (44.4 g.), Tween 85 (30.0 g.), and Mentor 28 (50.0 g.)
  2. 2
    その他reacted
  3. 3
    その他reached was 71° C.

実験手順

Acrylamide (AM) (49.6 g.), 2-methacryloyloxyethyl trimethyl ammonium methosulfate (METAMS) (26.0 g. of a 40% aqueous solution), distilled water (44.4 g.), Tween 85 (30.0 g.), and Mentor 28 (50.0 g.) were combined and reacted according to the procedure of Example 31. The pH of the emulsion was adjusted to 6.0; the maximum temperature reached was 71° C.; the product was a stable emulsion.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US04147681uspto-grants-1979_04