反応 #53832
ord-b3d31884ab3b488b93786e6af807f0d5
反応方程式
反応条件
詳細条件
See reaction.notes.procedure_details.
実験手順
In analogy to example 11.4, trans-[4-(4-Bromo-butoxy)-cyclohexyl]-methyl-amine hydrochloride and isobutyl chloroformate (with 2.1 eq N,N-diisopropylethylamine) were reacted to yield trans-[4-(4-Bromo-butoxy)-cyclohexyl]-methyl-carbamic acid isobutyl ester which was used directly in the next steps see Example 12.45-12.54.