反応 #53313

反応方程式

Triethylamine

Ethyl 4-(3-(2,6-dimethylbenzyloxy)phenyl)-4-bromobutyrate

→

title compound

Ethyl 4-(3-(2,6-dimethylbenzyloxy)phenyl)-3-butenoate

溶媒

carbon tetrachloride

反応条件

後処理

1. 1
   ろ過the mixture can be filtered through a pad of silica gel few times
2. 2
   濃縮concentrate

実験手順

Add Triethylamine to a solution of Ethyl 4-(3-(2,6-dimethylbenzyloxy)phenyl)-4-bromobutyrate (Step E) in carbon tetrachloride. After stirring approximately for 4 hours, the mixture can be filtered through a pad of silica gel few times, and concentrate to give the title compound.

出典