反応 #53227

ord-7fad1d254847413c8096c53b9b70c106

反応方程式

CCOC(=C1C(=O)Nc2ccccc21)c1ccccc1
3-(1-ethoxy-1-phenyl-methylidene)-2-indolinone
CN(C)CCS(=O)(=O)N(C)c1ccc(N)cc1
4-[N-(2-dimethylamino-ethylsulphonyl)-N-methyl-amino]-aniline
→
CN(C)CCS(=O)(=O)N(C)c1ccc(N/C(=C2\C(=O)Nc3ccccc32)c2ccccc2)cc1
(Z)-3-{1-[4-(N-(2-dimethylamino-ethylsulphonyl)-N-methyl-amino)-phenylamino]-1-phenyl-methylidene}-2-indolinone

反応物

CCOC(=C1C(=O)Nc2ccccc21)c1ccccc1
3-(1-ethoxy-1-phenyl-methylidene)-2-indolinone
CN(C)CCS(=O)(=O)N(C)c1ccc(N)cc1
4-[N-(2-dimethylamino-ethylsulphonyl)-N-methyl-amino]-aniline

試薬

なし

反応条件

詳細条件
See reaction.notes.procedure_details.

実験手順

Prepared analogously to Example 39 from 3-(1-ethoxy-1-phenyl-methylidene)-2-indolinone and 4-[N-(2-dimethylamino-ethylsulphonyl)-N-methyl-amino]-aniline.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US06855710B2uspto-grants-2005_02