反応 #531791

反応方程式

Mercaptopropionic acid

Triphenylmethylchloride

→

3-(tritylthio)propionic acid

収率 95.7%

溶媒

methylene chloride

反応条件

後処理

1. 1
   その他were carried out at room temperature
2. 2
   ろ過was gathered by filtration
3. 3
   その他the solid components obtained here
4. 4
   その他were dried under reduced pressure

実験手順

Mercaptopropionic acid 12 (3.14 g) was dissolved in 50 ml of methylene chloride. Triphenylmethylchloride 13 (8.36 g) was added to that, and 19-hour reactions were carried out at room temperature. The precipitate generated through the reactions was gathered by filtration, and the solid components obtained here were dried under reduced pressure, to form 9.86 g of 3-(tritylthio)propionic acid 14, which is a white solid.

出典