反応 #531788

反応方程式

1,3-bis(2,7,9-triphenyl-1,4,5,6-tetrahydropyrido[3,2-h]quinazolin-4-yl)benzene

→

1,3-bis(2,7,9-triphenylpyrido[3,2-h]quinazolin-4-yl)benzene

溶媒

diethyleneglycol

反応条件

後処理

1. 1
   温度was heated until total dissolution
2. 2
   温度the reaction was refluxed for 6 hours with argon bubbling directly in the solution

実験手順

A suspension of 1,3-bis(2,7,9-triphenyl-1,4,5,6-tetrahydropyrido[3,2-h]quinazolin-4-yl)benzene (5) (4.4 mmol) in 220 diethyleneglycol was heated until total dissolution. 1.2 g Pd/C was then slowly added, and the reaction was refluxed for 6 hours with argon bubbling directly in the solution. The reaction was then stopped, and the suspension cooled to room temperature.

出典