反応 #53163

ord-91440e6526c445f498c4dd830af6d05f

反応方程式

CS(=O)(=O)N(CC#N)c1ccc([N+](=O)[O-])cc1
N-cyanomethyl-N-methylsulphonyl-4-nitroaniline
→
CS(=O)(=O)N(CC#N)c1ccc(N)cc1
4-(N-cyanomethyl-N-methylsulphonyl-amino)-aniline

反応物

CS(=O)(=O)N(CC#N)c1ccc([N+](=O)[O-])cc1
N-cyanomethyl-N-methylsulphonyl-4-nitroaniline

試薬

なし

溶媒

CN(C)C=O
DMF

反応条件

詳細条件
See reaction.notes.procedure_details.

実験手順

Prepared analogously to Example 39c by catalytic hydrogenation of N-cyanomethyl-N-methylsulphonyl-4-nitroaniline in DMF.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US06855710B2uspto-grants-2005_02